Magnesium Glycerophosphate, Magnesium Gluconate Manufacturer Exporter

Annie Chemie P Ltd, is a company at Dahej in Gujarat, India. It is a manufacturer exporter of Magnesium Glycerophosphate & Magnesium Gluconate and oil field shale gas fracking or hydraulic fracturing chemicals and speciality chemicals and it has substantial exports to countries like USA, Canada, UK, Europe, UAE, Nigeria, Algeria, Turkey, Mexico, Brazil, Chile, Argentina, Australia, Kuwait, Dubai etc. We have developed encapsulated guar gel breaker based on coated ammonium persulfate, potassium persulfate, sodium persulfate, potassium peroxymonopersulfate, sodium bromate etc. We also supply other coated or encapsulated products like citric acid, guar crosslinkers other shale gas frac related products like diverting agent, KCl-substitute or clay-stabilizer, corossion inhibitors, scale inhibitor, bio-guard and several speciality chemicals.

Magnesium Glycerophosphate BP Ph Eur & Magnesium Gluconate USP BP Ph Eur FCC Food Grade Suppliers Exporters, Manufacturers

Magnesium Glycerophosphate
CAS Number: 927-20-8 BP Ph Eur Suppliers Exporters, Manufacturers
Magnesium Glycerophosphate Manufacturers Exporters

Magnesium Glycerophosphate Manufacturers Exporters

Magnesium Glycerophosphate BP Ph Eur Grade Specifications
Ph Eur
C3H7MgO6P -- 194.4 -- CAS 927-20-8

DEFINITION
Mixture, in variable proportions, of magnesium salts of (RS)-2,3-dihydroxypropyl phosphate and 2-hydroxy-1-(hydroxymethyl)ethyl phosphate, which may be hydrated.
Content: 11.0 per cent to 12.5 per cent of Mg (dried substance).

CHARACTERS
Appearance: White or almost white powder, hygroscopic.
Solubility: Practically insoluble in ethanol (96 per cent). It dissolves in dilute solutions of acids.

IDENTIFICATION
A. Mix 1 g with 1 g of potassium hydrogen sulphate in a test tube fitted with a glass tube. Heat strongly and direct the white vapour towards a piece of filter paper impregnated with a freshly prepared 10 g/l solution of sodium nitroprusside. The filter paper develops a blue colour in contact with piperidine.
B. Ignite 0.1 g in a crucible. Take up the residue with 5 ml of nitric acid and heat on a water-bath for 1 min. Filter. The filtrate gives reaction (b) of phosphates.
C. It gives the reaction of magnesium.

TESTS
Solution S: Dissolve 2.5 g in carbon dioxide-free water prepared from distilled water and dilute to 50 ml with the same solvent.
Appearance of solution: Solution S is not more opalescent than reference suspension.
Acidity: Dissolve 1.0 g in 100 ml of carbon dioxide-free water. Add 0.1 ml of phph solution. Not more than 1.5 ml of 0.1 M sodium hydroxide is required to change the colour of the indicator.
Glycerol and ethanol (96 per cent)-soluble substances: Maximum 1.5 per cent.
Shake 1.0 g with 25 ml of ethanol (96 per cent) for 2 min. Filter and wash the residue with 5 ml of ethanol (96 per cent). Combine the filtrate and the washings, evaporate to dryness on a water-bath and dry the residue at 70C for 1 h. The residue weighs a maximum of 15 mg.
Chlorides: Maximum 0.15 per cent.
Phosphates: Maximum 0.5 per cent.
Sulphates: Maximum 0.1 per cent.
Iron: Maximum 150 ppm.
Heavy metals: Maximum 20 ppm.
Loss on drying: Maximum 12.0 per cent, determined on 1.000 g by drying in an oven at 150C for 4 h.

Magnesium Gluconate
CAS Number: 3632-91-5 or 59625-89-7 for hydrate USP BP Ph Eur FCC Food Grade Suppliers Exporters, Manufacturers
Magnesium Gluconate Manufacturers Exporters

Magnesium Gluconate Manufacturers Exporters

Magnesium Gluconate USP Grade Specifications
C12H22MgO14xH2O -- (anhydrous) 414.60
D-Gluconic acid, magnesium salt (2:1), hydrate.
Magnesium D-gluconate (1:2) dihydrate 450.64 --- CAS 59625-89-7.
Anhydrous --- CAS 3632-91-5.

Magnesium Gluconate contains not less than 98.0 percent and not more than 102.0 percent of C12H22MgO14, calculated on the anhydrous basis.

Identification:
A: A solution (1 in 10) responds to the tests for Magnesium.
B: Chromatographic plate test.
pH: between 6.0 and 7.8, in a solution (1 in 20).
Water: between 3.0% and 12.0%.
Chloride: A 1.0-g portion shows no more chloride than corresponds to 0.70 mL of 0.020 N hydrochloric acid (0.05%).
Sulfate: A 2.0-g portion shows no more sulfate than corresponds to 1.0 mL of 0.020 N sulfuric acid (0.05%).
Heavy metals: the limit is 0.002%.
Reducing substances: the limit is 1.0%.

Magnesium Gluconate BP Ph Eur Grade Specifications
C12H22MgO14,xH2O --- 414.6 (anhydrous substance)

DEFINITION
Anhydrous or hydrated magnesium bis[(2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanoate] (anhydrous or hydrated magnesium di(D-gluconate)).
Content: 98.0 per cent to 102.0 per cent (anhydrous substance).

CHARACTERS
Appearance: White or almost white, amorphous, hygroscopic, crystalline or granular powder.
Solubility: Freely soluble in water, slightly soluble in ethanol (96 per cent), very slightly soluble in methylene chloride.

IDENTIFICATION
A. Thin-layer chromatography.
B. To 10 mL of solution S add 3 mL of ammonium chloride solution. A slight opalescence may be observed. Add 10 mL of disodium hydrogen phosphate solution. A white precipitate is formed that does not dissolve upon the addition of 2 mL of dilute ammonia.

TESTS
Solution S: Dissolve 1.0 g in water and dilute to 50 mL with the same solvent.
Appearance of solution: Solution S is clear and not more intensely coloured than the reference solution.
Sucrose and reducing sugars: Dissolve 0.5 g in a mixture of 2 mL of hydrochloric acid and 10 mL of water. Boil for 5 minutes, allow to cool, add 10 mL of sodium carbonate solution and allow to stand for 10 min. Dilute to 25 mL with water and filter. To 5 mL of the filtrate add 2 mL of cupri-tartaric solution and boil for 1 minute. Allow to stand for 2 minutes. No red precipitate is formed.
Chlorides: Maximum 500 ppm.
Sulfates: Maximum 500& ppm.
Water: Maximum 12 per cent, determined on 80 mg.
Microbial contamination:
TAMC: acceptance criterion 1000 CFU/g.
TYMC: acceptance criterion 100 CFU/g.

Magnesium Gluconate FCC Food Grade Specifications
[CH2OH(CHOH)4COO]2Mg
C12H22MgO14 Formula weight, anhydrous 414.60
C12H22MgO14-2H2O Formula weight, dihydrate 450.63
INS: 580 CAS: anhydrous 3632-91-5
CAS: dihydrate 59625-89-7

DESCRIPTION
Magnesium Gluconate occurs as a white to off white powder or granulate. It is anhydrous, the dihydrate, or a mixture of both. It is very soluble in water and is sparingly soluble in alcohol. It is insoluble in ether.

REQUIREMENTS
Identification
A. A 1:20 aqueous solution gives positive tests for Magnesium.
B. Chromatography Test.
Assay: Not less than 98.0% and not more than 102.0% of C12H22MgO14, calculated on the anhydrous basis.
Chloride: Not more than 0.05%.
Lead: Not more than 2 mg/kg.
Reducing Substances: Not more than 1.0%.
Sulfate: Not more than 0.05%.
Water: Between 3.0% and 12.0%.

Magnesium Glycerophosphate CAS Number 927-20-8 & Magnesium Gluconate CAS Number 3632-91-5 or 59625-89-7 for hydrate Supplier Exporter, Manufacturer:

Annie Chemie P Ltd
Mumbai 4000010, INDIA
With Agents and offices in UAE, USA, Europe.

Exporters to USA, Canada, UK, Europe, UAE, Nigeria, Algeria, Turkey, Mexico, Brazil, Chile, Argentina, Australia, Dubai etc.