Potassium Carbonate & Potassium Bicarbonate USP BP Ph Eur Analytical Reagent FCC Food Grade Suppliers Exporters, Manufacturers
Potassium Bicarbonate
CAS Number: 298-14-6 Suppliers Exporters, Manufacturers
Please visit Safety Data Sheet of Potassium Bicarbonate USP BP Ph Eur Analytical Reagent FCC Food Grade Manufacturers.
Potassium Bicarbonate USP Grade Specifications:
KHCO3 --- 100.12
Carbonic acid, monopotassium salt;
Monopotassium carbonate CAS 298-14-6DEFINITION
Potassium Bicarbonate contains NLT 99.5% and NMT 101.5% of KHCO3, calculated on the dried basis.IDENTIFICATION
A. Identification Tests - General, Potassium
B. Identification Tests - General, BicarbonateASSAY
Loss on Drying: Dry a sample over silica gel for 4 h: it loses NMT 0.3% of its weight.
Procedure
Sample: 4 g
Analysis: Dissolve the Sample in 100 mL of water, add methyl red TS, and titrate with 1 N hydrochloric acid. Add the acid slowly, with constant stirring, until the solution becomes faintly pink. Heat the solution to boiling, cool, and continue the titration until the pink color no longer fades after boiling. Each mL of 1 N hydrochloric acid is equivalent to 100.1 mg of KHCO3.
Acceptance criteria: 99.5% to 101.5% on the dried basis.
Normal Carbonate:
Sample: Grind 3.0 g of Potassium Bicarbonate with 25 mL of alcohol and 5 mL of water in a porcelain mortar.
Barium chloride solution: 12.216 mg/mL of barium chloride in alcohol and water (7:3), prepared by dissolving the barium chloride in water, then diluting with alcohol to final volume
Analysis: Add 3 drops of phenolphthalein to the Sample and titrate slowly with Barium chloride solution until the suspension becomes colorless. Continue the grinding for 2 min, and if the color turns pink, continue the titration with Barium chloride solution to a colorless endpoint. Repeat the grinding for 2 min and the addition of Barium chloride solution, if necessary, until the suspension is colorless after 2 min of grinding. Each mL of the barium chloride solution is equivalent to 6.911 mg of K2CO3.
Acceptance criteria: NMT 2.5%
Packaging and Storage: Preserve in well-closed containers.
Specifications of Potassium Bicarbonate BP
Potassium, Hydrogen Carbonate, Ph Eur
KHCO3 100.1 CAS 298-14-6DEFINITION
Content: 99.0 per cent to 101.0 per cent.CHARACTERS
Appearance: White or almost white, crystalline powder or colourless crystals.
Solubility: Freely soluble in water, practically insoluble in ethanol (96 per cent).
When heated in the dry state or in solution, it is gradually converted to potassium carbonate.IDENTIFICATION
A. To 5 mL of solution S (see Tests) add 0.1 mL of PhPh solution. A pale pink
colour is produced. Heat; gas is evolved and the colour becomes red.
B. It gives the reaction of carbonates and bicarbonates.
C. 1 mL of solution S gives reaction (b) of potassium.TESTS
Solution S: Dissolve 5.0 g in 90 mL of carbon dioxide-free water prepared from distilled water and dilute to 100 mL with the same solvent.
Appearance of solution: Solution S is clear and colourless.
Carbonates: The pH of freshly prepared solution S is not greater than 8.6.
Chlorides: Maximum 150 ppm.
Sulfates: Maximum 150 ppm.
Ammonium: Maximum 20 ppm.
Calcium: Maximum 100 ppm.
Iron: Maximum 20 ppm, determined on solution S.
Sodium: Maximum 0.5 per cent.
Atomic emission spectrometry: To pass the test.
Heavy metals: Maximum 10 ppm.
Specifications of Potassium Bicarbonate FCC Food Grade
KHCO3 Formula weight 100.12
INS: 501(ii) CAS: 298-14-6DESCRIPTION
Potassium Bicarbonate occurs as colorless, transparent, monoclinic prisms or as a white, granular powder. It is stable in air. Its solutions are neutral or alkaline to PhPh. One gram dissolves in 2.8 mL of water. It is almost insoluble in alcohol.
Function: pH control; leavening agent.REQUIREMENTS
Identification A 1:10 aqueous solution gives positive tests for Potassium and for Bicarbonate.
Assay: Not less than 99.0% and not more than 101.5% of KHCO3, calculated on the dried basis.
Carbonate: Passes test.
Lead: Not more than 2 mg/kg.
Loss on Drying: Not more than 0.25%.
Potassium Bicarbonate Analytical Reagent Grade
Potassium Hydrogen Carbonate
KHCO3
Formula Wt: 100.12
CAS Number: 298-14-6REQUIREMENTS
Assay (dried basis): 99.7-100.5% KHCO3MAXIMUM ALLOWABLE
Insoluble matter: 0.01%
Chloride (Cl): 0.001%
Phosphate (PO4): 5 ppm
Sulfur compounds (as SO4): 0.003%
Ammonium (NH4): 5 ppm
Heavy metals (as Pb): 5 ppm
Iron (Fe): 5 ppm
Calcium (Ca): 0.002%
Magnesium (Mg): 0.001%
Sodium (Na): 0.03%Please visit Hazard Statement of Potassium Bicarbonate USP BP Ph Eur Analytical Reagent FCC Food Grade Suppliers.
Potassium Carbonate
CAS Number: 584-08-7 USP BP Ph Eur Analytical Reagent FCC Food Grade Suppliers Exporters, Manufacturers
Please visit Safety Data Sheet of Potassium Carbonate USP BP Ph Eur Analytical Reagent FCC Food Grade Manufacturers.
Potassium Carbonate USP Grade Specifications:
K2CO3 (anhydrous) --- 138.21
K2CO3-1½ H2O --- 165.23
Carbonic acid, dipotassium salt;
Dipotassium carbonate CAS 584-08-7DEFINITION
Potassium Carbonate contains NLT 99.5% and NMT 100.5% of K2CO3, calculated on the dried basis.IDENTIFICATION
A. Identification Tests-General, Potassium: Meets the requirements
B. Identification Tests-General, Carbonate: Meets the requirements.ASSAY
Loss on Drying: Dry a sample at 180C for 4 h: it loses NMT 0.5% of its weight.
Procedure
Sample: Dried potassium carbonate obtained in the test for Loss on Drying
Analysis: Transfer the Sample to a flask with the aid of 150 mL of water and add 4 drops of methyl orange. Titrate with 1 N hydrochloric acid. Each mL of 1 N hydrochloric acid is equivalent to 69.11 mg of K2CO3.
Acceptance criteria: 99.5% to 100.5% on the dried basis
Insoluble Substances:
Sample solution: 1 g in 20 mL of water
Acceptance criteria: The solution is complete, clear, and colorless.
Packaging and Storage: Preserve in well-closed containers.
Specifications of Potassium Carbonate BP Grade
K2CO3DEFINITION
Content: 99.0 per cent to 101.0 per cent (dried substance).CHARACTERS
Appearance: White or almost white granular powder, hygroscopic.
Solubility: Freely soluble in water, practically insoluble in ethanol (96 per cent).IDENTIFICATION
A. Dissolve 1 g in 10 ml of water. The solution is strongly alkaline.
B. 2 ml of the solution prepared for identification test A gives the reaction of carbonates and bicarbonates.
C. 1 ml of the solution prepared for identification test A gives reaction of potassium.TESTS
Solution S: Dissolve 10.0 g in 25 ml of distilled water. Slowly add 14 ml of hydrochloric acid. When the effervescence has ceased, boil for a few minutes. Allow to cool and dilute to 50 ml with distilled water.
Appearance of solution: Solution S is not more opalescent than reference suspension and not more intensely coloured than reference solution.
Chlorides: Maximum 100 ppm.
Sulphates: Maximum 100 ppm.
Calcium: Maximum 100 ppm.
Iron: Maximum 10 ppm.
Heavy metals: Maximum 20 ppm.
Loss on drying: Maximum 5.0 per cent, determined on 0.300 g by drying in an oven at 120-125C for 5 h.
Specifications of Potassium Carbonate FCC Food Grade
K2CO3 Formula wt, anhydrous 138.21
K2CO3-1½H2O Formula wt, hydrated 165.23
INS: 501(i) CAS: 584-08-7DESCRIPTION
Potassium Carbonate is anhydrous or contains 1.5 molecules of water of crystallization. The anhydrous form occurs as a white, granular powder, and the hydrated form as small, white, translucent crystals or granules. It is very deliquescent, and its solutions are alkaline. One gram dissolves in 1 mL of water at 25C and in about 0.7 mL of boiling water. It is insoluble in alcohol.
Function: pH control.REQUIREMENTS
Identification: A 1:10 aqueous solution gives positive tests for Potassium and for Carbonate.
Assay: Not less than 99.0% and not more than 100.5% of K2CO3 after drying.
Insoluble Substances: Passes test.
Lead: Not more than 2 mg/kg.
Loss on Drying Anhydrous: Not more than 1%; Hydrated: Between 10.0% and 16.5%.
Specifications of Potassium Carbonate Anhydrous Analytical Reagent
Potassium Carbonate, Anhydrous
K2CO3
Formula Weight 138.21
CAS Number 584-08-7REQUIREMENTS
Assay: 99.0% K2CO3 minMAXIMUM ALLOWABLE
Insoluble matter: 0.01%
Chloride (as Cl): 0.003%
Nitrogen compounds (as N): 0.001%
Phosphate (PO4): 0.001%
Silica (SiO2): 0.005%
Sulfur compounds (as SO4): 0.004%
Ammonium hydroxide precipitate 0.01%
Heavy metals (as Pb): 5 ppm
Iron (Fe): 5 ppm
Calcium: 0.005%
Magnesium: 0.002%
Sodium (Na): 0.02%
Specifications of Potassium Carbonate Sesquihydrate Analytical Reagent
Potassium Carbonate Sesquihydrate
K2CO3 . 1.5H2O
Formula Wt 165.23
CAS Number 6381-79-9REQUIREMENTS
Assay: 98.5-101.0% K2CO3 . 1.5H2O
Loss on heating at 285C: 14.0-16.5%MAXIMUM ALLOWABLE
Insoluble matter: 0.01%
Chloride (as Cl): 0.003%
Nitrogen compounds (as N): 0.001%
Phosphate (PO4): 0.001%
Silica (SiO2): 0.005%
Sulfur compounds (as SO4): 0.004%
Ammonium hydroxide precipitate: 0.01%
Heavy metals (as Pb): 5 ppm
Iron (Fe): 5 ppm
Calcium (Ca): 0.005%
Magnesium (Mg): 0.002%
Sodium (Na): 0.02%.Please visit Hazard Statement of Potassium Carbonate USP BP Ph Eur Analytical Reagent FCC Food Grade Suppliers.
Potassium Bicarbonate CAS Number 298-14-6 & Potassium Carbonate CAS Number 584-08-7 Supplier Exporter, Manufacturer:
Annie Chemie P Ltd
Mumbai 4000010, INDIA
With Agents and offices in UAE, USA, Europe.e-mail: info@anniechemie.com
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