Sodium Bromide USP BP Ph Eur Analytical Reagent Grade & Sodium Bromate Suppliers Exporters, Manufacturers
Sodium Bromide
CAS Number: 7647-15-6 USP BP Ph Eur Analytical Reagent Grade Suppliers Exporters, Manufacturers
Please visit Safety Data Sheet of Sodium Bromide USP BP Ph Eur Analytical Reagent Grade Manufacturers.
Sodium Bromide USP Grade Specifications:
NaBr --- 102.89
Sodium bromide.
Sodium bromide --- CAS 7647-15-6Sodium Bromide contains not less than 98.0 percent and not more than 100.5 percent of NaBr, calculated on the dried basis. It contains no added substances.
Packaging and storage:Preserve in well-closed containers, and store at room tem perature.
Appearance of solution: clear and colorless.
Test solution: Dissolve 10.0 g in carbon dioxide-free water, and dilute with the same solvent to 100 mL.
Identification:
A: A solution containing 4.0 mg of sodium bromide responds to the test for Bromide.
B: It responds to the test for Sodium.
Acidity or alkalinity: To 10 mL of the solution prepared for the test for Appearance of solution, add 0.1 mL of bromothymol blue: not more than 0.5 mL of 0.01 N hydrochloric acid or 0.01 N sodium hydroxide is required to change the color of this solution.
Loss on drying: Dry it at 100C to 105C for 3 hours: it loses not more than 3.0% of its weight.
Bromates:
Starch-mercuric iodide solution: Triturate 1.0 g of soluble starch with 5 mL of water, and pour the mixture into 100 mL of boiling water containing 10 mg of mercuric iodide.
Procedure: To 10 mL of the solution prepared for the test for Appearance of solution add 1 mL of Starch–mercuric iodide solution, 0.1 mL of a 100 g per L solution of potassium iodide, and 0.25 mL of 0.5 M sulfuric acid. Allow to stand protected from light for 5 minutes. No blue or violet color develops.
Limit of chlorine: not more than 0.6%.
Iodides: To 5 mL of the solution prepared for the test for Appearance of solution add 0.15 mL of a 10.5 g per 100 mL ferric chloride solution, and 2 mL of dichloromethane. Shake, and allow to separate. The lower layer is colorless.
Sulfates: A 2.0-g portion shows no more sulfate than corresponds to 0.2 mL of 0.020 N sulfuric acid (0.01%).
Limit of iron: not more than 20 ppm.
Magnesium and alkaline-earth metals: To 200 mL of water add 0.1 g of hydroxylamine hydrochloride, 10 mL of pH 10.0 ammonia–ammonium chloride buffer (prepared by dissolving 5.4 g of ammonium chloride in 20 mL of water, adding 20 mL of ammonium hydroxide, and diluting to 100 mL), 1 mL of 0.1 M zinc sulfate, and about 0.2 g of eriochrome black T trituration. Heat to about 40C. Titrate this solution with 0.01 M edetate disodium until the violet color changes to deep blue. To this solution add 10.0 g of Sodium Bromide dissolved in 100 mL of water. If the color changes to violet, titrate the solution with 0.01 M edetate disodium to a deep blue endpoint. The volume of 0.01 M edetate disodium consumed in the second titration does not exceed 5.0 mL (0.02%, calculated as Ca).
Specifications of Sodium Bromide BP Ph Eur Grade
102.9 --- CAS 7647-15-6DEFINITION
Content: 98.5 per cent to 101.0 per cent (dried substance).CHARACTERS
Appearance: White or almost white, granular powder or small, colourless, transparent or opaque crystals, slightly hygroscopic.
Solubility: Freely soluble in water, soluble in ethanol (96 per cent).IDENTIFICATION
A. It gives reaction (a) of bromides.
B. Solution S (see Tests) gives the reactions of sodium.TESTS
Solution S: Dissolve 10.0 g in carbon dioxide-free water and dilute to 100 mL with the same solvent.
Appearance of solution: Solution S is clear and colourless.
Acidity or alkalinity: To 10 mL of solution S add 0.1 mL of bromothymol blue solution. Not more than 0.5 mL of0.01 M hydrochloric acid or 0.01 M sodium hydroxide is required to change the colour of the indicator.
Bromates: To 10 mL of solution S add 1 mL of starch solution, 0.1 mL of a 100 g/L solution of potassium iodide and 0.25 mL of 0.5 M sulfuric acid and allow to stand protected from light for 5 min. No blue or violet colour develops.
Chlorides and sulfates: Limits: chlorides: maximum 0.6 per cent; sulfates: maximum 0.01 per cent.
Iodides: To 5 mL of solution S add 0.15 mL of ferric chloride solution and 2 mL of methylene chloride. Shake and allow to separate. The lower layer is colourless.
Iron: Maximum 20 ppm.
Magnesium and alkaline-earth metals: Maximum 200 ppm, calculated as Ca.
Loss on drying: Maximum 3.0 per cent, determined on 1.000 g by drying in an oven at 105C for 3 h.
Sodium Bromide Analytical Reagent Grade
NaBr
Formula Weight: 102.89
CAS Number: 7647-15-6REQUIREMENTS
Assay (corrected): 99.0% NaBr
pH of a 5% solution: 5.0-8.8 at 25CMAXIMUM ALLOWABLE
Insoluble matter: 0.005%
Bromate (BrO3): 0.001%
Chloride (Cl): 0.2%
Nitrogen compounds (as N): 5 ppm
Sulfate (SO4): 0.002%
Barium (Ba): 0.002%
Heavy metals (as Pb): 5 ppm
Iron (Fe): 5 ppm
Calcium (Ca): 0.002%
Magnesium (Mg): 0.001%
Potassium (K): 0.1%.Please visit Hazard Statement of Sodium Bromide USP BP Ph Eur Analytical Reagent Grade Suppliers.
Sodium Bromate
CAS Number: 7789-38-0 Suppliers Exporters, Manufacturers
Please visit Safety Data Sheet of Sodium Bromate Manufacturers.
Specifications of Sodium Bromate
Description: White and Crystalline powder.
Appearance of 20% Aqueous Solution: Clear and colorless
Assay (on dry basis): 99.5% minimum.
pH of 5% Solution: 6-8%
Moisture by weight: 0.1% maximum.
Bromide: 0.06% maximum.
Chloride (as Cl): <0.1%
Sulfate: 0.03% maximum.
Iron (Fe): 0.0005% maximum.
Heavy Metals (as Pb): 0.0005% maximum.
Arsenic: 0.0005% maximum.
Insoluble matter: 0.003% maximum.Please visit Hazard Statement of Sodium Bromate Suppliers.
Sodium Bromide CAS Number 7647-15-6 & Sodium Bromate CAS Number 7789-38-0 Supplier Exporter, Manufacturer:
Annie Chemie P Ltd
Mumbai 4000010, INDIA
With Agents and offices in UAE, USA, Europe.e-mail: info@anniechemie.com
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September 30, 2023Exporters to USA, Canada, UK, Europe, UAE, Nigeria, Algeria, Turkey, Mexico, Brazil, Chile, Argentina, Australia, Dubai etc.
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